|
|
Line 30: |
Line 30: |
| | | |
| ===State diagram for the Basic GL processor=== | | ===State diagram for the Basic GL processor=== |
− |
| |
− | <table border=1 cellspacing=3 cellpadding=3>
| |
− | <th colspan=14>State diagram: Green = open valve, or power applied</th>
| |
− | <tr>
| |
− | <td>Step</td>
| |
− | <td>Heater</td>
| |
− | <td>Pump</td>
| |
− | <td>V1<sup><font color=red>1</font></sup></td>
| |
− | <td>V2</td>
| |
− | <td>V3</td>
| |
− | <td>V4</td>
| |
− | <td>V5</td>
| |
− | <td>V6</td>
| |
− | <td>V7</td>
| |
− | <td>Notes</td>
| |
− | </tr>
| |
− |
| |
− | <tr>
| |
− | <td>Oil in</td> <!-- Process Step -->
| |
− | <td color=green> </td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="on"> </td> <!-- Valve 1 -->
| |
− | <td class="off"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Pre-filtered</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Heat Oil</td> <!-- Process Step -->
| |
− | <td class="on"><font color=red>50C</font></td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Check level before applying heat</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Dewater oil</td> <!-- Process Step -->
| |
− | <td class="on"><font color=red>90C</font></td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="on"> </td> <!-- Valve 7 -->
| |
− | <td>Switch to 50C when O/P slows</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Cool oil</td> <!-- Process Step -->
| |
− | <td class="on">50C</td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="on"> </td> <!-- Valve 7 -->
| |
− | <td>Titrate oil now. Empty collector. I use NaOH</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Inject Methoxide</td> <!-- Process Step -->
| |
− | <td class="off"> </td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="on">Adj.</td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Allow 20 mins to inject.</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Reaction Stage</td> <!-- Process Step -->
| |
− | <td class="off"> </td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Allow 90 mins at 50C</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>5% Prewash</td> <!-- Process Step -->
| |
− | <td class="off"> </td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="on"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Mix 15 mins</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Settle Glycerol</td> <!-- Process Step -->
| |
− | <td class="off"> </td> <!-- Heater -->
| |
− | <td class="off"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="off"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Wait 90 mins</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Drain Glycerol</td> <!-- Process Step -->
| |
− | <td class="off"> </td> <!-- Heater -->
| |
− | <td class="off"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="on"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Drain slowly to avoid whirlpool</td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Distil methanol</td> <!-- Process Step -->
| |
− | <td class="on"><font color=red>90C</font></td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="off"> </td> <!-- Valve 5 -->
| |
− | <td class="on"> </td> <!-- Valve 6 -->
| |
− | <td class="on"> </td> <!-- Valve 7 -->
| |
− | <td></td> <!-- Notes -->
| |
− | </tr>
| |
− |
| |
− |
| |
− |
| |
− |
| |
− | <tr>
| |
− | <td>Drain Biodiesel </td> <!-- Process Step -->
| |
− | <td class="off">off</td> <!-- Heater -->
| |
− | <td class="on"> </td> <!-- Pump -->
| |
− | <td class="off"> </td> <!-- Valve 1 -->
| |
− | <td class="on"> </td> <!-- Valve 2 -->
| |
− | <td class="off"> </td> <!-- Valve 3 -->
| |
− | <td class="off"> </td> <!-- Valve 4 -->
| |
− | <td class="on">Adj.</td> <!-- Valve 5 -->
| |
− | <td class="off"> </td> <!-- Valve 6 -->
| |
− | <td class="off"> </td> <!-- Valve 7 -->
| |
− | <td>Ensure heater is OFF first! Caution - Hot! Wear breathing apparatus.<br>Take sample and perform 23/7 test before discharging whole batch.</td> <!-- Notes -->
| |
− | </tr>
| |
− | </table>
| |
| | | |
| | | |
This page is Work In Progress and therefore may not be complete.
|
Graham Laming with GL processor. Source GL
The GL Processor is a design by Graham Laming (hence the GL) and has probably become most popular processor design for homebrew biodiesel production in the UK. The processor features built in dewatering and Methanol recovery capabilities, as well as protection against user exposure to Methanol vapour. The design also lends itself to a variety of production techniques.
Basic design
The design has been in existence for many years. It has been supplemented and improved by various users during this time. Below is a schematic of Graham’s basic design (with sight glass added) along with instructions on its use. Reproduced with kind permission from Graham.
Although the design has been modified by others, Graham’s basic design is capable producing high quality Biodiesel and due to its simplicity of design is suitable for those new to home production.
This is a compact home made biodiesel processor which avoids water-washing and limits methanol release to very small amounts. You can also recover surplus Methanol from your biodiesel, which would otherwise be lost in the wash water.
You can de-water your oil in the processor and you can start to recover methanol from as low as 40 degrees C.
Here's a diagram of the system. It includes a simple venturi to recirculate vapour through a condenser. The venturi also sucks methoxide (or water, if you do the 5% prewash) from the methoxide container and mixes it into the oil flow.
Allow a straight horizontal run of around 30cm after the venturi outlet to ensure the venturi will perform properly. This is because the momentum of the out-flowing liquid acts to "pull" on the inlet vapour.
You can mount the Methoxide tank up, nearer the venturi, if your venturi's performance is marginal. Make sure it is not too high - you don't want to drop the container, spill the methoxide, or hurt your back.
State diagram for the Basic GL processor
Step |
Heater |
Pump |
V1 |
V2 |
V3 |
V4 |
V5 |
V6 |
V7 |
Notes |
Oil in |
|
|
|
|
|
|
|
|
|
Pre-filtered |
Heat Oil |
50°C |
|
|
|
|
|
|
|
|
Check level before applying heat |
Dewater oil |
90°C |
|
|
|
|
|
|
|
|
Switch to 50°C when O/P slows |
Cool oil |
50°C |
|
|
|
|
|
|
|
|
Titrate oil now. Empty collector. |
Inject Methoxide |
|
|
|
|
|
Adj. |
|
|
|
Allow 20 mins to inject. |
Reaction Stage |
|
|
|
|
|
|
|
|
|
Allow 90 mins at 50C |
5% Prewash |
|
|
|
|
|
|
|
|
|
Mix 15 mins |
Settle Glycerol |
|
|
|
|
|
|
|
|
|
Wait 90 mins |
Drain Glycerol |
|
|
|
|
|
|
|
|
|
Drain slowly to avoid whirlpool |
Distil methanol |
90°C |
|
|
|
|
|
|
|
|
Check level before applying heat |
Drain Biodiesel |
Off |
|
|
|
|
|
Adj. |
|
|
Ensure heater is OFF first! Caution - Hot! Wear breathing apparatus.
Take sample and perform 23/7 test before discharging whole batch. |