Keith,
Thanks for that. I've changed 5% to 7% and altered the much maligned GL processor page to reflect.
I know recent perceived wisdom states add Methoxide at full bore and have altered the GL page to suit. The reference to slow introduction on your page was only when using the pump suction for that purpose. I understand there is little chance of a spark especially with a brass impellor within a cast iron housing. However, I believe the mechanical seal relies, to a degree, on lubrication from the liquid being pumped and I'm uncertain as to the lubricating properties, if any, of Methoxide.
The seal is a source of friction and therefore possible heat and with the wrong combination of valves an inexperienced user could run the pump on pure Methoxide which I think should be avoided at all costs. I should, perhaps make it more obvious that the oil circulation should be running full bore and the Methoxide bled into this flow. Other than time, there are no issues in introducing the Methoxide slowly.
Thanks, although grossly misguided, I did cotton on to the jest! It pains me to admit that with the last two batches, in an attempt to eradicate HMPEs or what ever we are now calling the ones that don't liquefy until 30-40°C, I have pretty much emulated the procedure you use on your processor without the water wash, with apparent success.
I'm also wondering if all the bells and whistles I've spent time making are worthwhile. I spent ages making an adjustable squirrel which apparently speeded the distilling process when run with a tank temp of 85°C. However I found that when the squirrel was turned off and normal distilling continued at 85°C the distillation rate was the same!
Re the exposed heater issue, I pointed out the problem both on your design and on the GL (well, Graham did in his original text). It doesn't however, apply to Paddy's design, so in order to present the facts to newcomers I think it's only fair to point out these issues, especially where safety is concerned.
Good point re the wash tank, I'll try and word thing so that settling and bubbling can be used as alternatives. Maybe it would offer a more easily understood explanation if each had a separate page, any of which could be used in conjunction with your processor.
