Well the reaction is done, two stage non titraion, crystle clear 90/10 pass (with no jelly

).
The pump however didn't do quite so well, the immpeller has melted and eaten it's self.
Here are some picks
This is the spare set of immplers I had just in case.

and this is the set I've just tacken out




As you can see these PPO pumps just don't stand up to bio being demethed at 90°C
What's your looking like Tony ?