Here is a link to the ambient processing thread;
http://www.biopowered.co.uk/forum/index.php/topic,2442.msg30857.html#msg30857Maybe my figures on KOH usage are a little confusing on the thread so to clarify,
If I glyc wash 200 litres of oil with 60 litres of glycerol (from a friend that uses 20% methanol) then the wash alone with 5 litres of methanol added to the 60 litres produces around a 25% conversion.
The rest of the process will then complete in 1 or 2 stages with a total amount of 'about' 4.7gms/litre KOH and another 10% max added methanol (so total methanol usage of 12.5%
If my friends glycerol isn't available and I have to use my own with it's much lower excess amounts of KOH and methanol, I still add the 5 litres of methanol and get less conversion during the pre wash stage, something like 10% in which case the KOH total is more like 5.7gms. methanol usage is still a max of 12.5%
I have experimented with glyc washing at lower temps and it doesn't work as well. Which is why I use the M67 tank to do this.
Reaction times at ambient are only slightly longer, probably + 15 mins on each stage.
I add about 90% of the total expected KOH amount for stage 1 with 8% methanol. In the past if the conversion after the pre-wash has been high I have added only 6 to 7% methanol for stage 1 and used a total added amount of methanol of only 10.5%
I do realise it is impossible to get full conversion on this amount without the glycerol pre wash which extracts probably far more methanol and KOH than we realise, especially leaving it to mix at 60degs for 1 hour.