Author Topic: Titrated Acid water wash.  (Read 19940 times)

Offline nigelb

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Re: Titrated Acid water wash.
« Reply #45 on: February 06, 2013, 09:29:05 PM »
So if this is correct, and I suspect it is, demething the bio before washing could reduce the amount of washes needed.

How much methanol would you expect from the bio alone? Would the time and effort put in be outweighed by the volume recovered. Bare in mind the reduced methanol now being used in two stage no tit methods.... would it be worthwhile?
« Last Edit: February 06, 2013, 09:37:17 PM by nigelb »

Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #46 on: February 06, 2013, 09:31:03 PM »
I'm absolutely sure that a meth test on consequtive washes will show an incremental reduction everytime.

That would make sense, but it would be good to see if the soaps drop in a fairly linea way, if not is there a meth % that sees an increase in the amount of soaps released?  It would be an elegant answer to what can be seen from time to time, ie 50/50 clear on one wash, with the next wash producing a more cloudy 50/50.  It's not too important as going through HW shavings seems to do the job, but it's nice to be able to explain observations.


Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #47 on: February 06, 2013, 09:34:48 PM »
Demething does reduce water washing, but with new ways of pump washing with 2 or 3 buckets of water, is it worthwhile?

Steve, tried this I think prior to water washing?? I can't remember what he said about it.

Offline Head Womble

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Re: Titrated Acid water wash.
« Reply #48 on: February 06, 2013, 09:36:13 PM »
So if this is correct, and I suspect it is, demething the bio before washing could reduce the amount of washes needed.

How much methanol would you expect from the bio alone? Would the time and effort put in be outweighed by the volume recovered. Bare in mind the reduced the methanol now being used in two stage no tit methods would it be worthwhile?

It may not be worthwhile when doing non tit (I'm down to 16% meths now), but for others that are still titrating there may be some gains.
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Offline nigelb

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Re: Titrated Acid water wash.
« Reply #49 on: February 06, 2013, 09:37:56 PM »
Agreed

Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #50 on: February 06, 2013, 09:39:08 PM »
Jim

What are your conclusions about water washing?

Offline 1958steveflying

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Re: Titrated Acid water wash.
« Reply #51 on: February 06, 2013, 09:42:14 PM »
Demething does reduce water washing, but with new ways of pump washing with 2 or 3 buckets of water, is it worthwhile?

Steve, tried this I think prior to water washing?? I can't remember what he said about it.

The reason I was going to demeth before washing was simply because I was experiencing methanol fumes with every wash and even when the wash water was clear I got meth fumes when drying !

The next batch I made was with Acetone and it settled so quickly to a clear 50/50 I found it was not worth washing.

Offline Jamesrl

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Re: Titrated Acid water wash.
« Reply #52 on: February 06, 2013, 10:42:55 PM »

It may not be worthwhile when doing non tit (I'm down to 16% meths now), but for others that are still titrating there may be some gains.

I'm only using 10 - 11% virgin + ASM + reclaimed.

And yes I think demething IS worth the time and effort, less than 30p to get 4-5ltr of methanol back.

Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #53 on: February 07, 2013, 04:06:25 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

Offline Jamesrl

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Re: Titrated Acid water wash.
« Reply #54 on: February 07, 2013, 07:02:48 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

I partially dried the wet bio using the condenser AND squirrel and finished off in the settling tank with the Bubbler.

Offline Head Womble

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Re: Titrated Acid water wash.
« Reply #55 on: February 07, 2013, 07:31:52 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

I partially dried the wet bio using the condenser AND squirrel and finished off in the settling tank with the Bubbler.

Nothing new then.
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Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #56 on: February 07, 2013, 08:59:41 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

I partially dried the wet bio using the condenser AND squirrel and finished off in the settling tank with the Bubbler.

How long did this take?  The spray bar / ring thing dries in less than an hour.  In a sealed system it'd be good to have something comparable!

Offline 1958steveflying

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Re: Titrated Acid water wash.
« Reply #57 on: February 07, 2013, 09:30:58 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

I partially dried the wet bio using the condenser AND squirrel and finished off in the settling tank with the Bubbler.

How long did this take?  The spray bar / ring thing dries in less than an hour.  In a sealed system it'd be good to have something comparable!


Exactly the same system as most demeth with will work for drying mate.

Offline Rotary-Motion

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Re: Titrated Acid water wash.
« Reply #58 on: February 07, 2013, 09:44:23 PM »
i would just like to add i just read all this thread, i got nothing to offer, but all the same a very interesting read !

ok im done :)

Offline nathanrobo

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Re: Titrated Acid water wash.
« Reply #59 on: February 07, 2013, 10:13:10 PM »
James

Now you're potentially on board with us strange water washing types.  What can you do to shorten drying times in a sealed system (simplest possible method) to at least as comparable with a spray bar ring?

I partially dried the wet bio using the condenser AND squirrel and finished off in the settling tank with the Bubbler.

How long did this take?  The spray bar / ring thing dries in less than an hour.  In a sealed system it'd be good to have something comparable!


Exactly the same system as most demeth with will work for drying mate.

Cool!  On the new system then!