has anyone tried the technique yet?
I did tonight.
I glyc washed 160lt of pretty good oil.
I mixed 3.2lt of ASM and made up to 21lt with methanol and mixed for an hour.
I did a 90/10 and got just 0.6ml drop out.
Dropped the glyc and mixed it all up again.
Got 0.5ml drop out!

Mixed up another 0.3lt of ASM an 1.5lt of methanol and got a slightly hazy pass.
I was really hoping that the mix following the glyc drop from stage 1 would send the reaction to completion. Ah well!
Like Julian said earlier in this thread....negative results are worthy of publication and discussion too.
Nige