Author Topic: My bio at different temp's.  (Read 1539 times)

Offline Manfred

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My bio at different temp's.
« on: March 07, 2014, 12:42:51 PM »
I usually only process oil that's been stood in my settling tank or creamed off the top of my cubies. However I picked a batch up off the bay, left it a fortnight on the back, thought it looked ok so upended 90 Ltrs into my processor. Using NaOH @ 5g/ ltr 1st stage then 4g/ltr 2nd stage. Mixed 1 hour no fallout on 10/90. Water wash then dried then bubble for 18 hours. All looked ok.



 Next day when I switched off the bubbler.
URL=http://s1157.photobucket.com/user/miketheknite/media/Bio/image.jpg.html][/URL]

So I put it into the freezer.





URL=http://s1157.photobucket.com/user/miketheknite/media/Bio/image-2.jpg.html][/URL]

At 6'C it melted back to clear Usable Bio.
I have run all winter with my usual process with no additive, just shows what can happen when you aren't careful.


Offline Julian

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Re: My bio at different temp's.
« Reply #1 on: March 07, 2014, 02:12:50 PM »
Nothing really untoward.

Swirly bits are typical of what everyone calls HMPE when formed in a sealed jar.

Your freezer will be around -18°C photos are typical of waxing/gelling, quite normal at that sort of temperature.

Just hang on to the fuel till the weather gets a little bit warmer and it will be perfectly OK to use.
Used Cooking Oil Collection website ... http://www.surreyusedcookingoilcollection.palmergroup.co.uk

Offline Manfred

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Re: My bio at different temp's.
« Reply #2 on: March 07, 2014, 02:34:15 PM »
Thank's Julian. I'e got 2 weeks of stock so not in a rush and the weather is  starting to look promising. ( fingers crossed )

Offline Tony

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Re: My bio at different temp's.
« Reply #3 on: March 07, 2014, 02:51:02 PM »
That swirly one is all too familiar.  Definitely my winter nemesis :)

Offline Julian

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Re: My bio at different temp's.
« Reply #4 on: March 07, 2014, 03:05:30 PM »
I should have said ... top photo of finished bio is good looking stuff.
Used Cooking Oil Collection website ... http://www.surreyusedcookingoilcollection.palmergroup.co.uk