Biopowered - vegetable oil and biodiesel forum

Biodiesel => Chemistry and process => Topic started by: nigelb on November 18, 2012, 05:23:20 PM

Title: Next batch!
Post by: nigelb on November 18, 2012, 05:23:20 PM
Is anybody making a batch anytime soon. I won't be making any til next weekend probably and will be trying out a new twist on current methods. If anyone wants to try it out let me know via the message service and I'll let you know what it involves. I don't want to discuss it in the open forum as I've not tried it myself.

Nige
Title: Re: Next batch!
Post by: Tony on November 18, 2012, 06:20:35 PM
Hi Nige, yes probably within a few days mate, drop me a PM :)
Title: Re: Next batch!
Post by: Carrington on November 18, 2012, 06:26:39 PM
Hi Nigel
I could maybe have a small go on the bench , is it chemistry or process that is the twist

Paul
Title: Re: Next batch!
Post by: julesandtash on November 18, 2012, 06:56:14 PM
Damn, just drying a batch now so too late. I will do another next weekend though.
Title: Re: Next batch!
Post by: nigelb on November 18, 2012, 07:53:52 PM
The only reason I don't want anything published openly, is that the possible change in chemistry is not my idea and I've not trialed it myself. If I had and found positive results then I would not have any problems in opening it up for discussion.
Title: Re: Next batch!
Post by: nigelb on November 18, 2012, 07:56:12 PM
Jules, Julian, Carrington, Tony, Keith and Will.....you all have messages
Title: Re: Next batch!
Post by: Julian on November 18, 2012, 08:09:32 PM
The only reason I don't want anything published openly, is that the possible change in chemistry is not my idea and I've not trialed it myself. If I had and found positive results then I would not have any problems in opening it up for discussion.

Negative results are equally worthy of discussion though.
Title: Re: Next batch!
Post by: nigelb on November 18, 2012, 08:15:58 PM
Yes..I totally agree Julian.

Nige
Title: Re: Next batch!
Post by: Head Womble on November 18, 2012, 09:33:10 PM
Nige can you PM me the details too please.

I've just finished a batch but have oil settling ready for the next one.
Title: Re: Next batch!
Post by: Julian on November 18, 2012, 10:00:46 PM
Don't tell him, Nige ... it's meant t be a secret and besides he steals concrete mixers!
Title: Re: Next batch!
Post by: photoman290 on November 18, 2012, 10:05:56 PM
Don't tell him, Nige ... it's meant t be a secret and besides he steals concrete mixers!

anyone asked heston blumemthal if he makes bio. he likes his concrete mixers.
Title: Re: Next batch!
Post by: Julian on November 18, 2012, 10:40:49 PM
And barrows, he steals wheel barrows too.
Title: Re: Next batch!
Post by: Head Womble on November 18, 2012, 10:43:22 PM
And barrows, he steals wheel barrows too.

I've got your float as well, you forgot about that didn't you.
Title: Re: Next batch!
Post by: Carrington on November 18, 2012, 10:48:24 PM


I've got your float as well, you forgot about that didn't you.
[/quote]

Is that a wooden/ plastic float or a steel trowel
Title: Re: Next batch!
Post by: Julian on November 18, 2012, 10:49:55 PM
Ahhh, my float ... I remember my float.  It's been so long since I've seen her. We used to have such fun together, but now she's ...
Title: Re: Next batch!
Post by: Julian on November 18, 2012, 10:50:32 PM


I've got your float as well, you forgot about that didn't you.

Is that a wooden/ plastic float or a steel trowel
[/quote]

Been so long I can't remember ... I loose all my tools this way.
Title: Re: Next batch!
Post by: Head Womble on November 18, 2012, 10:59:18 PM
Ahhh, my float ... I remember my float.  It's been so long since I've seen her. We used to have such fun together, but now she's ...

Um, maybe I should just drop it on your doorstep, ring the bell and drive off.
I don't need to see the reunion of a man and his tool, that's the sort of stuff that nightmares are made of.
Title: Re: Next batch!
Post by: Rotary-Motion on November 19, 2012, 11:02:50 AM
just knowing where they are is enough  :)
Title: Re: Next batch!
Post by: Julian on November 19, 2012, 12:08:40 PM
just knowing where they are is enough  :)

No, he'll have them on ebay as soon as he thinks I've forgotten about them.
Title: Re: Next batch!
Post by: Head Womble on November 19, 2012, 09:36:16 PM
just knowing where they are is enough  :)

No, he'll have them on ebay as soon as he thinks I've forgotten about them.

Forget Ebay, it's to tracable.
I'll be weighing them in.
Title: Re: Next batch!
Post by: nigelb on November 23, 2012, 10:04:46 PM
has anyone tried the technique yet?

I did tonight.

I glyc washed 160lt of pretty good oil.

I mixed 3.2lt of ASM and made up to 21lt with methanol and mixed for an hour.

I did a 90/10 and got just 0.6ml drop out.

Dropped the glyc and mixed it all up again.

Got 0.5ml drop out! :(

Mixed up another 0.3lt of ASM an 1.5lt of methanol and got a slightly hazy pass.

I was really hoping that the mix following the glyc drop from stage 1 would send the reaction to completion. Ah well!

Like Julian said earlier in this thread....negative results are worthy of publication and discussion too.

Nige

Title: Re: Next batch!
Post by: julesandtash on November 24, 2012, 03:19:59 PM
I tried it too. I made the first stage with the normal amount of chemicals then, after draining the first stage glycerol I mixed for an hour with no added chemicals. It made no difference at all - the fallout at the end was the same as at the start of the hour.
It took the calculated amount of second stage chemicals to get a clear pass.
Title: Re: Next batch!
Post by: Glycer-rides on November 24, 2012, 05:47:41 PM
I tried that earlier this year just after I started doing the 2 stage no tit, but to try and push a failed S2 forward.

As said, no dice. Worth a go for the small effort required.